NiFe1 . 98Nd0 . 02O4-Fe 双层吸波涂层设计及制备

张泽洋, 张海丰, 燕艳, 刘祥萱, 李伟

表面技术 ›› 2014, Vol. 43 ›› Issue (4) : 119-123.

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PDF(4174 KB)
表面技术 ›› 2014, Vol. 43 ›› Issue (4) : 119-123.
应用技术

NiFe1 . 98Nd0 . 02O4-Fe 双层吸波涂层设计及制备

  • 张泽洋1, 张海丰1, 燕艳1, 李伟1, 刘祥萱2
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Design and Preparation of Double-layer Microwave Absorbers Based on Carbonyl Iron and NiFe1 . 98Nd0 . 02O4

  • ZHANG Ze-yang1, ZHANG Hai-feng1, YAN yan1, LI Wei1, LIU Xiang-xuan2
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摘要

目的 制备高性能 NiFe1 . 98Nd0 . 02O4-Fe 双层吸波涂层。 方法 采用溶胶凝胶自燃烧法制备钕掺杂 NiFe1 . 98Nd0 . 02O4。 借助 X 射线衍射仪、扫描电镜和矢量网络分析仪对 NiFe1 . 98Nd0 . 02O4 和羰基铁的结构、形貌、电磁参数进行测试分析。 采用遗传算法对 NiFe1 . 98Nd0 . 02O4-羰基铁双层涂层的厚度进行优化设计。 结果 以环氧树脂为基体,以羰基铁和 NiFe1 . 98Nd0 . 02O4 为吸波剂的双层吸波涂层具备较好的吸波性能,厚度约 1 mm,反射率在 9 . 25 ~ 11 . 35 GHz 范围内均小于-10 dB。 结论 NiFe1 . 98Nd0 . 02O4 层和羰基铁层在吸波性能上有很好的互补性,理论优化结果和实验结果相同。

Abstract

Objective To prepare high-performance double-absorbing coating NiFe1 . 98Nd0 . 02O4 -Fe. Methods Nd substituted nickel ferrites ( NiFe1 . 98Nd0 . 02O4 ) were prepared using the sol-gel-autocombustion method. The microstructures, morphology and the electromagnetic properties of NiFe1 . 98Nd0 . 02O4 and carbonyl iron were characterized with X-ray diffraction ( XRD) , scanning electron microscopy ( SEM) and a vector network analyzer. The thickness of double-layers microwave absorption coating was optimized by the genetic algorithm ( GA) . Results Using carbonyl iron and NiFe1 . 98Nd0 . 02O4 as absorbents, double composite absorbing coating with thickness d = 1 mm was prepared. The results showed that the reflection loss of coating was less than-10 dB over the range from 9. 25 GHz to 11. 35 GHz. Conclusion The results of measurements showed that the microwave absorption property of NiFe1 . 98Nd0 . 02O4 and carbonyl iron were complementary to each other. The calculated RL agreed closely with the experimental results in the whole measured frequency range.

关键词

钕掺杂; 双层吸波涂层; 反射率; 吸波性能

Key words

Nd substitution; double-layers absorber; reflectivity; microwave absorbing property

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张泽洋, 张海丰, 燕艳, 刘祥萱, 李伟. NiFe1 . 98Nd0 . 02O4-Fe 双层吸波涂层设计及制备[J]. 表面技术. 2014, 43(4): 119-123
ZHANG Ze-yang, ZHANG Hai-feng, YAN yan, LIU Xiang-xuan, LI Wei. Design and Preparation of Double-layer Microwave Absorbers Based on Carbonyl Iron and NiFe1 . 98Nd0 . 02O4[J]. Surface Technology. 2014, 43(4): 119-123

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