张宇,李庆,曹金利,覃礼钊,张进,李元,戴策.室温水溶液法制备 Cu2O 纳米颗粒及其光催化性能[J].表面技术,2013,42(3):75-77.
ZHANG Yu,LI Qing,CAO Jin-li,QIN Li-zhao,ZHANG Jin,LI Yuan,DAI Ce.Synthesis of Cu2O Nano-particles by Solution Methods at Room-temperature and Their Photocatalytic Performances[J].Surface Technology,2013,42(3):75-77 |
| 室温水溶液法制备 Cu2O 纳米颗粒及其光催化性能 |
| Synthesis of Cu2O Nano-particles by Solution Methods at Room-temperature and Their Photocatalytic Performances |
| 投稿时间：2013-01-31 修订日期：2013-03-10 |
| DOI： |
| 中文关键词: 氧化亚铜 纳米材料 光催化性能 |
| 英文关键词:cuprous oxide nanophase materials photocatalytic performance |
| 基金项目:重庆市自然科学基金重点项目( cstc2012jjB50011) ;重庆市高校新材料开发及应用研究创新团队建设项目( 201042 ) ;中央高校基本科研业务费专项资金( XDJK2011C064) |
| 作者 | 单位 |
| 张宇 | 西南大学 材料科学与工程学院, 重庆 400715 |
| 李庆 | 西南大学 材料科学与工程学院, 重庆 400715 |
| 曹金利 | 西南大学 材料科学与工程学院, 重庆 400715 |
| 覃礼钊 | 西南大学 材料科学与工程学院, 重庆 400715 |
| 张进 | 重庆文理学院 重庆市高校微纳米材料工程与技术重点实验室, 重庆 402160 |
| 李元 | 西南大学 材料科学与工程学院, 重庆 400715 |
| 戴策 | 西南大学 材料科学与工程学院, 重庆 400715 |
|
| Author | Institution |
| ZHANG Yu | School of Materials Science and Engineering, Southwest University, Chongqing 400715 , China |
| LI Qing | School of Materials Science and Engineering, Southwest University, Chongqing 400715 , China |
| CAO Jin-li | School of Materials Science and Engineering, Southwest University, Chongqing 400715 , China |
| QIN Li-zhao | School of Materials Science and Engineering, Southwest University, Chongqing 400715 , China |
| ZHANG Jin | Key Laboratory of Micro / nano Materials Engineering and Technology of Chongqing Colleges and Universities,Chongqing School of Arts and Sciences, Chongqing 402160 , China |
| LI Yuan | School of Materials Science and Engineering, Southwest University, Chongqing 400715 , China |
| DAI Ce | School of Materials Science and Engineering, Southwest University, Chongqing 400715 , China |
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| 中文摘要: |
| 以乙酸铜为铜源,茁-环糊精为表面活性剂,NaOH 为添加剂,KBH4 为还原剂,在室温水溶液中制备了直径约为 50 nm 的 Cu2O,对产物的组成、能隙、光催化性能进行了分析。 研究表明:产物结晶性良好,粒径分布较均匀,且产率高;此外,该纳米 Cu2O 由于比表面积大,对甲基橙在 30 min 内的催化效率高达 94 . 9% ,甲基橙几乎全部被降解,显示出良好的催化活性。 |
| 英文摘要: |
| With copper acetate as copper source, beta cyclodextrin as surfactant, NaOH as additive and KBH4 as reducing agent, the cuprous oxide nanoparticles with a diameter of about 50 nm were prepared in aqueous solution at room temperature. The composition, energy gap and photocatalytic performance of the products were analyzed. The study showed that the products had uniform particle size distribution, good crystallinity and high yield. As the as-prepared Cu2O nanoparticles had a larger surface area, the catalytic efficiency on methyl orange was about 94 . 9 % in 30 min, almost all methyl orange was degradated, showing that the product had a good photocatalytic activity. |
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