微波诱导羟基磷灰石 / 钛合金界面反应的研究

夏海滨, 王贻宁, 王爱华, 黄朝, 吴宇

表面技术 ›› 2013, Vol. 42 ›› Issue (1) : 53-55,74.

PDF(3766 KB)
PDF(3766 KB)
表面技术 ›› 2013, Vol. 42 ›› Issue (1) : 53-55,74.
研究与探索

微波诱导羟基磷灰石 / 钛合金界面反应的研究

  • 夏海滨1, 王贻宁1, 王爱华2, 吴宇2, 黄朝3
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Study on Hydroxyapatite / Titanium Alloy Interface Reaction Induced by Microwave

  • XIA Hai-bin1, WANG Yi-ning1, WANG Ai-hua2, WU Yu2, HUANG Zhao3
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摘要

为改善钛合金和 HA 涂层的界面相容性,采用电泳法在钛合金表面预先沉积均匀的 HA 涂层,再于 1200 ℃ 下进行微波处理。 通过对涂层相结构的分析,证明在微波诱导作用下,形成了梯度结构的涂层。 梯度过渡层由 TiO2 和 TiO 组成的致密氧化层、CaTiO3 和微量 HA 组成,能够缓解 HA 涂层与钛合金热膨胀系数不匹配的问题,减少涂层开裂,提高涂层与基体的结合强度。

Abstract

In order to improve the interface compatibility between titanium alloys and hydroxyapatite ( HA) coating, a uniform HA coating was fabricated by electrophoretic deposition firstly, then the coating was treated in microwave at 1200 ℃ .Through the analyzing the phase structure of the coating, it is proved that a gradient coating is obtained by microwave inducement . The gradient coating is composed of oxide layer with TiO2and TiO, CaTiO3and a minute amount of HA. Because the gradient structure can alleviate the mismatch of thermal expansion coefficient between HA and titanium alloys, less cracks and higher bonding strength can be obtained.

关键词

羟基磷灰石; 钛合金; 电泳沉积; 微波诱导; 界面反应

Key words

hydroxyapatite; titanium alloy; electrophoretic deposition; microwave inducement; interface reaction

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夏海滨, 王贻宁, 王爱华, 黄朝, 吴宇. 微波诱导羟基磷灰石 / 钛合金界面反应的研究[J]. 表面技术. 2013, 42(1): 53-55,74
XIA Hai-bin, WANG Yi-ning, WANG Ai-hua, HUANG Zhao, WU Yu. Study on Hydroxyapatite / Titanium Alloy Interface Reaction Induced by Microwave[J]. Surface Technology. 2013, 42(1): 53-55,74

基金

国家“973冶 项目(2012CB619600)

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