| WANG Jing-yan,ZHANG De-qiu,MU Li-ting,HE Xin,LI Mu-qin.Corrosion Resistance of Chitosan/Chlorogenic Acid Composite Coating Prepared by Electrophoretic Deposition[J],50(6):85-92 |
| Corrosion Resistance of Chitosan/Chlorogenic Acid Composite Coating Prepared by Electrophoretic Deposition |
| Received:May 15, 2021 Revised:June 02, 2021 |
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| DOI：10.16490/j.cnki.issn.1001-3660.2021.06.008 |
| KeyWord:magnesium electrophoretic deposition ultrasonic micro-arc oxidation chlorogenic acid corrosion resistance |
| Author | Institution |
| WANG Jing-yan |
Key Lab of Oral Biomedical Materials and Clinical Application of Heilongjiang Province;Engineering Research Center of the Ministry of Education on Metal Wear Resistant Materials and Surface Technology, School of Materials Science and Engineering, Jiamusi University, Jiamusi , China |
| ZHANG De-qiu |
Key Lab of Oral Biomedical Materials and Clinical Application of Heilongjiang Province;Engineering Research Center of the Ministry of Education on Metal Wear Resistant Materials and Surface Technology, School of Materials Science and Engineering, Jiamusi University, Jiamusi , China |
| MU Li-ting |
Key Lab of Oral Biomedical Materials and Clinical Application of Heilongjiang Province;Engineering Research Center of the Ministry of Education on Metal Wear Resistant Materials and Surface Technology, School of Materials Science and Engineering, Jiamusi University, Jiamusi , China |
| HE Xin |
Key Lab of Oral Biomedical Materials and Clinical Application of Heilongjiang Province;Engineering Research Center of the Ministry of Education on Metal Wear Resistant Materials and Surface Technology, School of Materials Science and Engineering, Jiamusi University, Jiamusi , China |
| LI Mu-qin |
Key Lab of Oral Biomedical Materials and Clinical Application of Heilongjiang Province;Engineering Research Center of the Ministry of Education on Metal Wear Resistant Materials and Surface Technology, School of Materials Science and Engineering, Jiamusi University, Jiamusi , China |
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| Abstract: |
| In order to improve the corrosion resistance and biological activity of pure magnesium, chlorogenic acid extracted from traditional Chinese medicine was deposited on ultrasonic micro-arc oxidation surface by electrophoretic deposition. The surface morphology and organizational structure of various samples were studied by scanning electron microscopy, X-ray diffractometer, atomic force microscopy, X-ray photoelectron spectroscopy, fourier transform infrared spectroscopy and contact angle measuring instrument. The corrosion behavior and resistance of various samples were also studied and evaluated. The main phase composition of UMAO/CS/CA coating is Mg, MgO and Mg2SiO4, and the main elemental compositions are O, C, Mg, Si and N. The stretching vibration peaks of O—H, aromatic hydrocarbon bonds, C==O bonds and benzene rings appear in CA coating. Chinese herbal extract and chitosan are mainly combined by chemical binding and physical adsorption. The UMAO/CS/CA coating is a hydrophobic surface, the contact angle of that is 104.1°. Electrochemical corrosion experiments show that the corrosion current density (Jcorr) of Mg is 1.7569×10−5 A/cm2 in simulated body fluid (SBF) environment. Among them, the icorr of UMAO/CS/CA coating is 3.767×10−6 A/cm2, which reduced by at least one order of magnitude compared to that of Mg. UMAO/CS/CA coating can better induce calcium and phosphor deposition. The UMAO/CS/CA coating can not only reduce the contact area between the corrosion solution and the coating surface, but also isolate the ions in the solution, which is difficult to be wetted by SBF, and can provide more effective protection for the magnesium matrix. UMAO/CS/CA coating has excellent biological activity. |
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