WANG Yin-chu,LI De-liang,DONG Ming-qi,XU Yu-xia.Influencing Factors of Low Concentration Cuprous' Measure[J],39(5):107-110
Influencing Factors of Low Concentration Cuprous' Measure
Received:June 10, 2010  Revised:October 10, 2010
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KeyWord:low concentration cuprous  influencing factors  orthogonal experiment  acidic etcher
           
AuthorInstitution
WANG Yin-chu College of Materials Science& Engineering,Central South University of Forestry and Technology, Changsha , China
LI De-liang College of Materials Science& Engineering,Central South University of Forestry and Technology, Changsha , China
DONG Ming-qi College of Materials Science& Engineering,Central South University of Forestry and Technology, Changsha , China
XU Yu-xia College of Materials Science& Engineering,Central South University of Forestry and Technology, Changsha , China
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Abstract:
      In order to establish the optimal measure conditions of low concentration cuprous contentin acidic etcher solution to improve work efficiency, titrimetry with cerium sulfate was used to study the influence of several factors on measure results by single factors, and combine with orthogonal experiment, the best results was obtained of several In- fluence factors.The results show that the influence of titration time, the concentration of HCl, joined volume of FeCl3, measure temperature and sample volume on measure results are outstanding, but the content of Cu2+ is indistinctively; And measured the solution that concentration of cuprous is 5 g/ L, and could finish in the 5 minutes and normal temperature, the relative error is- 0.8% when the concentration of HCl is 7 mol/ L, joined volume of FeCl3in the measure process is 10 mL and sample volume of solution is 10 mL.
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