| LIU Wen-ke,CAO Xiao-hua,PENG Shu-ming,LONG Xing-gui,YANG Ben-fu,LUO Shun-zhong,WANG Wei-du.Preparation of Anode Oxidation Layer on the Surface of Titanium Film and its Surface Property[J],36(1):51-55 |
| Preparation of Anode Oxidation Layer on the Surface of Titanium Film and its Surface Property |
| Received:September 11, 2006 Revised:February 10, 2007 |
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| DOI： |
| KeyWord:Titanium film Anode oxidation Preparation Surface property |
| Author | Institution |
| LIU Wen-ke |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
| CAO Xiao-hua |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
| PENG Shu-ming |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
| LONG Xing-gui |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
| YANG Ben-fu |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
| LUO Shun-zhong |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
| WANG Wei-du |
Institute of Nuclear Physics and Chemistry, China Academy of Engineering Physics, Mianyang , China |
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| Abstract: |
| It was necessary that anode oxidation layers are prepared on the surface of titanium film and its surface property is ascertained for the sake of investigating effects of anodic oxide layers on characteristics of absorbing and desorbing hydrogen isotope. Anodic oxidation apparatus on the surface of titanium film of molybdenum substrate is designed. The technical parameters of anodic oxidation what determine the thickness of anode oxidation layers are ascertained. The AES profile and XPS valency analysis of anode oxidation layer are measured. The results indicate that the color anode oxidation layers are prepared by using anodic oxidation apparatus designed and machined in the ascertained technical parameters of anodic oxidation, the oxidation technique is simple, and operated easily. The surface of the anode oxidation layers is flat, slick and uniform, and the anode oxidation layers link firmly with titanium films. The anode oxidation layers thicken with the increasing of voltage, concentration of H2SO4 and time respectively when other condition is uniform. Titanium valency on the surface of oxide layers is analyzed by XPS, and its result shows that titanium valency mainly is +4, ＋3 and +2 .The component is TiO2, Ti2O3 and TiO mainly in the anode oxidation layers. |
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