薛燕,王振国.沉积时间对AZ91D合金表面Ni-P-SiC复合镀层性能的影响[J].表面技术,2017,46(7):91-96.
XUE Yan,WANG Zhen-guo.Effect of Deposition Time on Properties of Ni-P-SiC Composite Coating on AZ91D Alloy[J].Surface Technology,2017,46(7):91-96 |
| 沉积时间对AZ91D合金表面Ni-P-SiC复合镀层性能的影响 |
| Effect of Deposition Time on Properties of Ni-P-SiC Composite Coating on AZ91D Alloy |
| 投稿时间：2017-01-22 修订日期：2017-07-20 |
| DOI：10.16490/j.cnki.issn.1001-3660.2017.07.015 |
| 中文关键词: AZ91D镁合金 Ni-P-SiC复合镀层 厚度 表面粗糙度 腐蚀 磨损 |
| 英文关键词:AZ91D magnesium alloy Ni-P-SiC composite plating thickness surface roughness corrosion wear |
| 基金项目:国家自然科学基金（51401027） |
| 作者 | 单位 |
| 薛燕 | 重庆工程职业技术学院，重庆 402260 |
| 王振国 | 北京航空航天大学，北京 100091 |
|
| Author | Institution |
| XUE Yan | Chongqing Vocational Institute of Engineering, Chongqing 402260, China |
| WANG Zhen-guo | Beihang University, Beijing 100191, China |
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| 中文摘要: |
| 目的 提高镁合金的耐蚀性和耐磨性。方法 以AZ91D镁合金为基体，采用SiC颗粒质量浓度为3 g/L的Ni-P化学镀溶液，在其表面沉积不同时间，制备Ni-P-SiC复合镀层。通过扫描电子显微镜（SEM）、显微硬度测试、粗糙度仪、电化学腐蚀和磨损等试验来分析和评价Ni-P-SiC复合镀层的厚度、表面粗糙度、显微硬度、耐腐蚀性能和耐磨性能。结果 Ni-P-SiC复合镀层的厚度和表面粗糙度随沉积时间增加而增加，沉积时间为150 min时，镀层厚度可达53 μm，表面粗糙度为2.5 μm。沉积时间为120 min时，镀层的显微硬度最高，为641HV，此时复合镀层的耐蚀性和耐磨性最好，自腐蚀电位高达−0.73 V，腐蚀电流密度为0.78 µA/cm2，磨损体积最小，为1.04×10−3 mm3。与AZ91D镁合金基体相比，沉积复合镀层后的样品更耐蚀，说明复合镀层有效改善了镁合金基体的耐蚀性。结论 沉积时间对Ni-P-SiC复合镀层的性能有一定影响，在沉积时间为120 min时获得的复合镀层具有较好的耐蚀性和耐磨性。 |
| 英文摘要: |
| The work aims to enhance corrosion and wear resistance of magnesium alloys. Ni-P-SiC composite coating was prepared by depositing AZ91D magnesium alloy in Ni-P electroless plating solution with 3 g/L SiC particle for different deposition time. Thickness, surface roughness, microhardness, wear and corrosion resistance of Ni-P-SiC composite coating were analyzed and evaluated with SEM, roughmeter, electrochemical corrosion and wear tests. The thickness and surface roughness of Ni-P-SiC composite coating increased as deposition time increased. When the deposition time was 150 min, the thickness and roughness were 53 μm and 2.5 μm, respectively; when the deposition time was 120 min, the maximum microhardness was 641HV, corrosion and wear resistance were the best, Ecorr, Jcorr and wear volume were −0.73 V, 0.78 µA/cm2 and 1.04×10−3 mm3, respectively. Compared with the AZ91D magnesium alloy, the sample produced after deposition exhibited better corrosion resistance after deposition, indicating that the Ni-P-SiC composite coating has improved corrosion resistance of the Mg alloy effectively. The properties of Ni-P-SiC composite coating are significantly influenced by deposition time. And the composite coating obtained at the deposition time of 120 min has better corrosion and wear resistance. |
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