LIU Tao,LIU Ying,DI Yue-lan,WANG Hai-dou,ZHENG Bo-yuan.Preparation and Hydrophobic Mechanism Analysis of 3Cr13 Stainless Steel Surface with Micro-Nano Structure[J],49(7):112-119
Preparation and Hydrophobic Mechanism Analysis of 3Cr13 Stainless Steel Surface with Micro-Nano Structure
Received:October 22, 2019  Revised:July 20, 2020
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DOI:10.16490/j.cnki.issn.1001-3660.2020.07.014
KeyWord:3Cr13 stainless steel  sand blasting  chemical etching  hydrophobic property  morphology
              
AuthorInstitution
LIU Tao 1.School of Mechatronics Engineering, Nanchang University, Nanchang , China; 2.Key Laboratory of National Defense Science and Technology for Equipment Remanufacturing Technology, Academy of Army Armored Forces, Beijing , China
LIU Ying 1.School of Mechatronics Engineering, Nanchang University, Nanchang , China
DI Yue-lan 2.Key Laboratory of National Defense Science and Technology for Equipment Remanufacturing Technology, Academy of Army Armored Forces, Beijing , China
WANG Hai-dou 2.Key Laboratory of National Defense Science and Technology for Equipment Remanufacturing Technology, Academy of Army Armored Forces, Beijing , China
ZHENG Bo-yuan 2.Key Laboratory of National Defense Science and Technology for Equipment Remanufacturing Technology, Academy of Army Armored Forces, Beijing , China; 3.School of Engineering and Technology, China University of Geosciences Beijing, Beijing , China
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Abstract:
      Stainless steel is a widely used engineering material and improving its hydrophobic property can provide self-cleaning property and reduce corrosion. Parameters such as the size and quantity of surface morphology have an important influence on the contact angle. The work aims to construct the micro-nano structure of 3Cr13 stainless steel with hydrophobic property to analyze the relationship between the mcro-nano structure and hydrophobic property. Besides, a two-step method combining sandblasting and chemical etching was designed. The micro-nano surface of 3Cr13 stainless steel with hydrophobic property was prepared by optimizing different parameters of sand blasting and chemical etching processes. The difference between the surface microstructure of hydrophilic and hydrophobic samples was inferred from the surface morphology parameters, and the prediction was proved from the different area distribution of the microstructure. The surface of stainless steel substrate was distributed by micro-nano structures composed of micro-pores and nano-particles. Sandblasting and etching parameters affected the roughness factors on the micro-nano structure of the substrate. The size and distribution of the surface micro-pores affected the hydrophobic property. The ratio of 200~1000 μm2 pores to the total pores area on the surface of hydrophobic samples was more than 39%, while the ratio of the pores larger than 1000 μm2 to the total pores area was less than 30%. That was to say, the surface micro-structures of hydrophobic samples were mostly composed of dense small pores. By sandblasting and chemical etching, the surface of 3Cr13 stainless steel can produce micro-nano double structure with hydrophobic property, and the hydrophobic property is closely related to the area of microstructure. When the area of pore above 1000 μm2 is less than 30%, the sample is hydrophobic.
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