史周琨,徐丽萍,张吉阜,肖根升,邓春明,宋进兵,刘敏,胡永俊.HVOF制备铝青铜涂层工艺优化及工艺参数对涂层性能的影响[J].表面技术,2021,50(8):101-108.
SHI Zhou-kun,XU Li-ping,ZHANG Ji-fu,XIAO Gen-sheng,DENG Chun-ming,SONG Jin-bing,LIU Min,HU Yong-jun.Optimization of Preparation Process of Aluminum Bronze Coating by HVOF and Effect of Process Parameters on Coating Properties[J].Surface Technology,2021,50(8):101-108
HVOF制备铝青铜涂层工艺优化及工艺参数对涂层性能的影响
Optimization of Preparation Process of Aluminum Bronze Coating by HVOF and Effect of Process Parameters on Coating Properties
投稿时间:2020-09-16  修订日期:2020-12-11
DOI:10.16490/j.cnki.issn.1001-3660.2021.08.010
中文关键词:  铝青铜涂层  铝合金  超音速火焰喷涂  工艺优化  极差分析法  正交实验
英文关键词:aluminum bronze coating  aluminum alloy  HVOF  process optimization  range ananlysis  orthogonal experimental
基金项目:国家重点研发计划(2017YFB0306100);广东特支计划(2019BT02C629)
作者单位
史周琨 广东工业大学 材料与能源学院,广州 510006;广东省科学院新材料研究所 a.现代材料表面工程技术国家工程实验室 b.广东省现代表面工程技术重点实验室,广州 510651 
徐丽萍 广东省科学院新材料研究所 a.现代材料表面工程技术国家工程实验室 b.广东省现代表面工程技术重点实验室,广州 510651 
张吉阜 广东省科学院新材料研究所 a.现代材料表面工程技术国家工程实验室 b.广东省现代表面工程技术重点实验室,广州 510651 
肖根升 中国航发湖南动力机械研究所,湖南 株洲 412002 
邓春明 广东省科学院新材料研究所 a.现代材料表面工程技术国家工程实验室 b.广东省现代表面工程技术重点实验室,广州 510651 
宋进兵 广东省科学院新材料研究所 a.现代材料表面工程技术国家工程实验室 b.广东省现代表面工程技术重点实验室,广州 510651 
刘敏 广东省科学院新材料研究所 a.现代材料表面工程技术国家工程实验室 b.广东省现代表面工程技术重点实验室,广州 510651 
胡永俊 广东工业大学 材料与能源学院,广州 510006 
AuthorInstitution
SHI Zhou-kun School of Materials and Energy, Guangdong University of Technology, Guangzhou 510006, China;a.National Engineering Laboratory for Modern Materials Surface Engineering Technology, b.the Key Lab of Guangdong for Modern Surface Engineering Technology, Guangdong Institute of New Materials, Guangzhou 510651, China 
XU Li-ping a.National Engineering Laboratory for Modern Materials Surface Engineering Technology, b.the Key Lab of Guangdong for Modern Surface Engineering Technology, Guangdong Institute of New Materials, Guangzhou 510651, China 
ZHANG Ji-fu a.National Engineering Laboratory for Modern Materials Surface Engineering Technology, b.the Key Lab of Guangdong for Modern Surface Engineering Technology, Guangdong Institute of New Materials, Guangzhou 510651, China 
XIAO Gen-sheng AECC Hunan Aviation Powerplant Research Institute, Zhuzhou 412002, China 
DENG Chun-ming a.National Engineering Laboratory for Modern Materials Surface Engineering Technology, b.the Key Lab of Guangdong for Modern Surface Engineering Technology, Guangdong Institute of New Materials, Guangzhou 510651, China 
SONG Jin-bing a.National Engineering Laboratory for Modern Materials Surface Engineering Technology, b.the Key Lab of Guangdong for Modern Surface Engineering Technology, Guangdong Institute of New Materials, Guangzhou 510651, China 
LIU Min a.National Engineering Laboratory for Modern Materials Surface Engineering Technology, b.the Key Lab of Guangdong for Modern Surface Engineering Technology, Guangdong Institute of New Materials, Guangzhou 510651, China 
HU Yong-jun School of Materials and Energy, Guangdong University of Technology, Guangzhou 510006, China 
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中文摘要:
      目的 利用超音速火焰喷涂技术,在铸铝表面沉积质量优良的铝青铜涂层。方法 基于正交实验,研究煤油流量、氧气流量、送粉速率和喷涂距离对涂层厚度、孔隙率、显微硬度和结合强度的影响。通过XRD图谱,对喷涂粉末和涂层相结构组成进行分析。利用场发射扫描电子显微镜,观察涂层截面形貌,测量涂层厚度。使用ImageJ软件测量孔隙率。采用显微硬度计和电子万能试验机,测量涂层的显微硬度和结合强度。针对正交实验结果,采用极差分析法进行分析,确定最优的工艺参数。结果 由极差法分析得到最优工艺参数:煤油流量为22 L/h,氧气流量为900 L/min,送粉速率为80 g/min,喷涂距离为200 mm。采用最优工艺参数制备涂层,测得涂层厚度为405.43 μm,孔隙率为0.10%,结合强度为61.63 MPa,显微硬度为330.33HV0.3。结论 与粉末相比,涂层的相组成未发生改变,均为α相和β′相。通过极差分析可知,不同工艺参数对涂层孔隙率、厚度、显微硬度和结合强度的影响程度不同。在本实验选取的主要工艺参数中,送粉速率对涂层孔隙率和厚度的影响程度最大,喷涂距离对涂层显微硬度的影响程度最大,煤油流量对结合强度的影响程度最大。
英文摘要:
      In order to obtain aluminum bronze coating with excellent coating quality on cast aluminum surface by High Velocity Oxygen Fuel spraying technology, the effects of kerosene flux, oxygen flux, powder feeding rate and spraying distance on coating thickness, porosity, microhardness and bonding strength are studied based on orthogonal experiment. The phase composition of the spray powder and coatings is analyzed by XRD. The cross-section morphology of the coating is observed by SEM, and the coating thickness is measured. The porosity is measured by ImageJ. The microhardness and bonding strength of the coating are measured by micro hardness tester and electronic universal testing machine. Range analysis method is used to analyze the results of orthogonal experiment to determine the optimal process parameters. It is obtained by range analysis that the optimal process parameters are kerosene flux 22 L/h, the oxygen flux 900 L/min, the powder feeding rate 80 g/min, and the spraying distance 200 mm. The coating thickness is 405.43 μm, the porosity is 0.10%, the bonding strength is 61.63 MPa, and the microhardness is 330.3 HV0.3 when the optimal process is adopted. The results show that the phase composition of the spray powder and coating is the same, both of which are α phase and β' phase. According to the range analysis table, different process parameters have different effects on the porosity, thickness, microhardness and bonding strength of the coating. The powder feeding rate has the greatest influence on the coating thickness and porosity, the spraying distance has the greatest influence on the micro hardness of the coating, and the kerosene flux has the greatest influence on the bonding strength.
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