余剑武,陆岳托,罗红,仝瑞庆,宋金根.基于微铣削的微结构尺寸与形状对PMMA表面疏水性的影响[J].表面技术,2021,50(1):287-295.
YU Jian-wu,LU Yue-tuo,LUO Hong,TONG Rui-qing,SONG Jin-gen.Effects of Dimension and Shape of Micro-milled Microstructure on PMMA Surface Hydrophobicity[J].Surface Technology,2021,50(1):287-295
基于微铣削的微结构尺寸与形状对PMMA表面疏水性的影响
Effects of Dimension and Shape of Micro-milled Microstructure on PMMA Surface Hydrophobicity
投稿时间:2020-01-06  修订日期:2020-11-30
DOI:10.16490/j.cnki.issn.1001-3660.2021.01.024
中文关键词:  微结构  表面疏水性  接触角  钉扎效应  微铣削
英文关键词:microstructure  surface hydrophobicity  contact angle  pinning effect  micro-milling
基金项目:国家自然科学基金项目(51275165,51575174);长沙市科技项目(kq1801007)
作者单位
余剑武 湖南大学 机械与运载工程学院,长沙 410082;汽车车身先进设计制造国家重点实验室,长沙 410082 
陆岳托 湖南大学 机械与运载工程学院,长沙 410082 
罗红 湖南大学 机械与运载工程学院,长沙 410082;汽车车身先进设计制造国家重点实验室,长沙 410082 
仝瑞庆 湖南大学 机械与运载工程学院,长沙 410082 
宋金根 湖南大学 机械与运载工程学院,长沙 410082 
AuthorInstitution
YU Jian-wu School of Mechanical and Vehicle Engineering, Hunan University, Changsha 410082, China;State Key Laboratory of Advanced Design and Manufacturing for Vehicle Body, Changsha 410082, China 
LU Yue-tuo School of Mechanical and Vehicle Engineering, Hunan University, Changsha 410082, China 
LUO Hong School of Mechanical and Vehicle Engineering, Hunan University, Changsha 410082, China;State Key Laboratory of Advanced Design and Manufacturing for Vehicle Body, Changsha 410082, China 
TONG Rui-qing School of Mechanical and Vehicle Engineering, Hunan University, Changsha 410082, China 
SONG Jin-gen School of Mechanical and Vehicle Engineering, Hunan University, Changsha 410082, China 
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中文摘要:
      目的 研究不同微结构尺寸参数和阵列形状对PMMA表面疏水性的影响。方法 使用精密微铣削方式,在光滑PMMA表面加工微沟槽、方柱、圆形及椭圆形阵列,并将测量的水滴的接触角和形状作为表面疏水性的表征指标。结果 当微沟槽阵列的微槽宽度B、凸台宽度C及微槽深度H分别在84.86~208.77 μm、36.22~133.94 μm、63.76~136.60 μm变化时,垂直接触角θ⊥分别在129.4°~143.5°、138.3°~124.0°、125.8°~141.8°变化,平行接触角θ∥分别在62.3°~69.6°、75.0°~66.3°、81.5°~72.0°变化;当微方柱阵列的BCH分别在70.76~138.99 μm、47.52~128.04 μm、70.84~175.94 μm变化时,接触角θ分别在130.3°~102.1°、114.9°~129.5°、105.7°~119.7°变化。水滴在微沟槽和椭圆形阵列表面的形状为椭球冠状,在微方柱和圆形阵列表面为球冠状。结论 微结构尺寸参数和阵列形状对PMMA表面疏水性有不同影响,且θ⊥的变化都比θ∥的变化更为明显。钉扎效应对水滴的形状有很大的影响,对于微沟槽阵列的槽垂直方向和椭圆形、圆形阵列,钉扎效应对水滴的形状起主导作用;对于微沟槽阵列的槽平行方向和微方柱阵列,水滴形状则受钉扎效应与固液气三相接触线不连续性的共同影响。研究结果有望为设计功能可控仿生微结构提供技术支撑。
英文摘要:
      The work aims to investigate the effects of different dimensions and array shapes of microstructure on PMMA surface hydrophobicity. Microgroove, square-pillar, circular and elliptical arrays were prepared on PMMA surface through precision micro-milling. The measured contact angle and shape of water droplet were used to indicate the surface hydrophobicity. When the microgroove width B, the boss width C, and the microgroove depth H of the microgroove arrays changed from 84.86 to 208.77 μm, 36.22 to 133.94 μm and 63.76 to 136.60 μm, the vertical contact angle θ⊥ changed from 129.4° to 143.5°, 138.3° to 124.0° and 125.8° to 141.8°, and the parallel contact angle θ∥ varied from 62.3° to 69.6°, 75.0° to 66.3°, and 81.5° to 72.0°, respectively. When the B, C, and H of the micro square-pillar arrays changed from 70.76 to 138.99 μm, 47.52 to 128.04 μm and 70.84 to 175.94 μm, the contact angle θ changed from 130.3° to 102.1°, 114.9° to 129.5°, and 105.7° to 119.7°, respectively. Water droplets showed elliptical droplet shape on the surfaces of microgroove and elliptical arrays, while the spherical shape on the micro square-pillar and circular arrays. The dimensions and array shapes of microstructures have different effects on the surface hydrophobicity of PMMA and the θ⊥ is more sensitive to the change of dimensions than θ∥. Moreover, the shape of water droplet is obviously influenced by pinning effect. On elliptical and circular arrays and perpendicular direction of microgroove arrays, the shape of water droplets is dominated by pinning effect. However, on the micro square-pillar arrays and the parallel direction of microgroove arrays, the shape of the water droplet is controlled by the pinning effect and the discontinuity of the solid-liquid-gas three-phase contact line. Research results are expected to support the design of the bio-functional microstructure surfaces.
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