黄珂,杨伏良,陈力学,马凯,郭磊.痕法测定 TiAlN 涂层结合强度的研究[J].表面技术,2013,42(5):107-111.
HUANG Ke,YANG Fu-liang,CHEN Li-xue,MA Kai,GUO Lei.Study on the Adhesion Strength of a TiAlN Coating by Scratch Tester[J].Surface Technology,2013,42(5):107-111 |
| 痕法测定 TiAlN 涂层结合强度的研究 |
| Study on the Adhesion Strength of a TiAlN Coating by Scratch Tester |
| 投稿时间：2013-04-16 修订日期：2013-05-22 |
| DOI： |
| 中文关键词: 磁控溅射 TiAlN 涂层 结合强度 |
| 英文关键词:magnetron sputtering TiAlN coating adhesion strength |
| 基金项目:国家“863冶 高新技术研究资助项目(2011AA030101) ;湖南省自然科学基金项目(12JJ3038) |
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| Author | Institution |
| HUANG Ke | School of Materials Science and Engineering, Central South University, Changsha 410083 , China;Key Laboratory of Nonferrous Metal Materials Science and Engineering, Ministry of Education Central South University, Changsha 410083 ,China |
| YANG Fu-liang | School of Materials Science and Engineering, Central South University, Changsha 410083 , China;Key Laboratory of Nonferrous Metal Materials Science and Engineering, Ministry of Education Central South University, Changsha 410083 ,China |
| CHEN Li-xue | Changsha Shenhu Ion Plating Ltd. , Changsha 410030 , China |
| MA Kai | School of Materials Science and Engineering, Central South University, Changsha 410083 , China;Key Laboratory of Nonferrous Metal Materials Science and Engineering, Ministry of Education Central South University, Changsha 410083 ,China |
| GUO Lei | School of Materials Science and Engineering, Central South University, Changsha 410083 , China;Key Laboratory of Nonferrous Metal Materials Science and Engineering, Ministry of Education Central South University, Changsha 410083 ,China |
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| 中文摘要: |
| 采用磁控溅射法在不锈钢表面制备了 TiAlN 涂层,采用压入法及划痕法表征了涂层的结合强度。分析表明,压入法只能作为一种定性的测定方法,该法测得 TiAlN 涂层的结合强度达到 HF3 。 划痕法结合了声信号、摩擦力信号和划痕微观形貌,可以定量测定结合强度,该法测得在压头曲率半径为 200 滋m 的情况下, TiAlN涂层的临界载荷达到 13 N,比传统 TiN 涂层提高了 45% 。 |
| 英文摘要: |
| TiAlN coating was prepared on the surface of stainless steel by magnetron sputtering mothed. Indentation and scratch test was used to investigated the adhesion strength of the coating. Results show that the indentation test is only a qualitative test method, and the adhesion strength measured by indentation test reaches HF3 . The results of scratch test show that it is combination of AE signal, frictional force signal and scratch micromorphology. It is a quantitative method for test adhesive strength. When the radius of the Rockwell indenter is 0 . 2 mm, the critical load of TiAlN coating is 13 N, contrast with the traditional TiN coating, the adhesion strength of TiAlN increased by 45 % . |
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