窦雯雯,牛玉超,黄国威,徐勇,王献忠,王孝丽,张琳琳.酸碱复合催化溶胶-凝胶法制备 SiO2减反膜及膜性能研究[J].表面技术,2013,42(1):63-66.
DOU Wen-wen,NIU Yu-chao,HUANG Guo-wei,XU Yong,WANG Xian-zhong,WANG Xiao-li,ZHANG Lin-lin.Preparation of SiO2Anti-reflective Coatings by Acid / Base Composite Catalyzed Sol-gel Method and Research on Their Properties[J].Surface Technology,2013,42(1):63-66
酸碱复合催化溶胶-凝胶法制备 SiO2减反膜及膜性能研究
Preparation of SiO2Anti-reflective Coatings by Acid / Base Composite Catalyzed Sol-gel Method and Research on Their Properties
投稿时间:2012-09-13  修订日期:2012-09-27
DOI:
中文关键词:  溶胶-凝胶  酸碱复合催化  SiO2 减反膜  透过率  表面形貌
英文关键词:Sol-gel  acid / base composite catalyzed  SiO2anti-reflective coating  transmissivity  surface morphology
基金项目:山东省科技发展计划(2010G0020318) ;山东省自然科学基金( ZR2010EM062 ) ;济南市高校自主创新计划( 201004048 ) ;山东省教育厅科技计划( J12LA12)
作者单位
窦雯雯 山东建筑大学 材料科学与工程学院, 济南 250101 
牛玉超 山东建筑大学 材料科学与工程学院, 济南 250101 
黄国威 山东建筑大学 材料科学与工程学院, 济南 250101 
徐勇 山东建筑大学 材料科学与工程学院, 济南 250101 
王献忠 山东建筑大学 材料科学与工程学院, 济南 250101 
王孝丽 山东建筑大学 材料科学与工程学院, 济南 250101 
张琳琳 山东建筑大学 材料科学与工程学院, 济南 250101 
AuthorInstitution
DOU Wen-wen School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
NIU Yu-chao School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
HUANG Guo-wei School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
XU Yong School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
WANG Xian-zhong School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
WANG Xiao-li School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
ZHANG Lin-lin School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101 , China 
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中文摘要:
      采用酸催化法、碱催化法和酸碱复合催化法制备了 SiO2 溶胶,进而制得 SiO2 减反膜。 表征了薄膜的表面形貌,测定了薄膜的透射率和硬度。 结果表明,不同催化溶胶制得的膜层在表面形貌、减反效果和薄膜硬度等方面存在明显差异:酸催化得到的薄膜,孔隙率和透过率最低,但硬度和抗划伤性最好;碱催化得到的薄膜,孔隙率和透过率最高,但硬度和抗划伤性最差;酸碱复合催化得到的薄膜,孔隙率、透过率、硬度和抗划伤性能介于以上二者之间,性能与酸碱复合催化溶胶的制备工艺密切相关。
英文摘要:
      The SiO2sol and anti-reflective coatings were prepared by the acid, base, and acid / base composite catalyzed methods. The surface morphologies of coatings were characterized and their transmissivity and hardness were measured .The experiments results show that, the surface morphology, anti-reflective effect and hardness of the coatings from three sols are very different; The coating from acid-catalyzed sol has the minimum porosity, lowest transmissivity, but highest hardness and best scratch resistance; The coating from ammonia-catalyzed sol gets maximum porosity, highest transmissivity, but lowest hardness and worst scratch resistance; The properties of the coatings from acid / base composite catalyzed sol are between those of the coatings by acid and base catalyzed sol-gel process like porosity, transmissivity, hardness, and scratch resistance performance.These properties will be directly affected by acid / base composite catalyzed sol-gel process.
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